Steroidal lactones from withania somnifera

72) Shanks DJ, et al. The efficacy of selamectin in the treatment of naturally acquired infestations of sarcoptes scabiei on dogs. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):269-81.

73) McTier TL, et al. Prevention of experimentally induced heartworm (Dirofilaria immitis) infections in dogs and cats with a single topical application of selamectin. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):259-68.

74) Boy MG, et al. Efficacy and safety of selamectin against fleas and heartworms in dogs and cats presented as veterinary patients in North America. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):233-50.

75) Shanks DJ, et al. Efficacy of selamectin in the treatment and prevention of flea (Ctenocephalides felis felis) infestations on dogs and cats housed in simulated home environments. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):213-22.

76) McTier TL, et al. Evaluation of the effects of selamectin against adult and immature stages of fleas (Ctenocephalides felis felis) on dogs and cats. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):201-12.

77) Bishop BF, et al. Selamectin: a novel broad-spectrum endectocide for dogs and cats. In: Veterinary Parasitology. 2000 Aug 23;91(3-4):163-76.

Cuscohygrine (along with the related metabolite hygrine) was first isolated by Carl Liebermann in 1889 as an alkaloid accompanying cocaine in coca leaves (also known as Cusco-leaves). Cuscohygrine is an oil that can be distilled without decomposition only in vacuum. It is soluble in water. It also forms a crystalline trihydrate, which melts at 40–41 °C. There are also the alkaloids ashwagandhine, ashwaganidhine, and somniferine, all of which have been identified exclusively in the ashwagandha plant itself. [ citation needed ]

Steroid isolation , depending on context, is the isolation of chemical matter required for chemical structure elucidation, derivitzation or degradation chemistry, biological testing, and other research needs (generally milligrams to grams, but often more [38] or the isolation of "analytical quantities" of the substance of interest (where the focus is on identifying and quantifying the substance (for example, in biological tissue or fluid). The amount isolated depends on the analytical method, but is generally less than one microgram. [39] [ page needed ] The methods of isolation to achieve the two scales of product are distinct, but include extraction , precipitation, adsorption , chromatography , and crystallization . In both cases, the isolated substance is purified to chemical homogeneity; combined separation and analytical methods, such as LC-MS , are chosen to be "orthogonal"—achieving their separations based on distinct modes of interaction between substance and isolating matrix—to detect a single species in the pure sample. Structure determination refers to the methods to determine the chemical structure of an isolated pure steroid, using an evolving array of chemical and physical methods which have included NMR and small-molecule crystallography . [2] : 10–19 Methods of analysis overlap both of the above areas, emphasizing analytical methods to determining if a steroid is present in a mixture and determining its quantity. [39]

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Steroidal lactones from withania somnifera

steroidal lactones from withania somnifera

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